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Why crystallite size decrease with increasing temperature
WebMar 15, 2015 · The crystallite size L is calculated by the Scherrer equation: (4) L = k λ β cos θ where k is a geometrical Scherrer constant ( k = 0.94); λ is the X-ray wave length (for Cu radiation λ = 1.54 Å); β is the intensity of full width at half maximum (FWHM); and θ is the Bragg angle ( Guérin & Alvarez, 1995 ). 3. Results and discussion 3.1. WebSep 22, 2006 · X-ray diffraction (XRD) shows there is crystallite size enlargement as bath temperature increases. The band gap energy values, determined from optical reflectance spectra, are between 3.2 and 3.3 eV, decreasing when the bath temperature increases. WebFeb 1, 2016 · CdS thin films deposited at different bath temperature and different concentration of buffer salt in CBD bath, such as a1, a2 and a3 samples. The growth parameters affected the thin films properties such as the crystallite size, compositional, optical and optoelectrical properties. The crystallite size decreased as the nucleation … eastman steel flex washing machine hose